tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium

Base Information

Chemical Name:tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium
CAS No.:122846-94-0
Molecular Formula:C₂₄H₂₃CrNO₆
Molecular Weight:473.446
Hs Code.:

Synonyms:tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium

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Chemical Property of tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium

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Technology Process of tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium

There total 1 articles about tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1122-58-3
dmap

: 24424-99-5
di-tert-butyl dicarbonate

: 29160-36-9
pentacarbonyl[(methoxy)(4-methylphenyl)carbene]chromium(0)

: 100-46-9
benzylamine

: 121809-50-5
pentacarbonyl(DMAP)chromium

: 122846-94-0
tetracarbonyl{(N-((2,2-dimethylethoxy)carbonyl)-N-(phenylmethyl)amino)(4-methylphenyl)methylene-C,O}chromium

Guidance literature:: In diethyl ether; byproducts: HO2COC(CH3)3, CO; under N2; dropwise addn. of benzylamine to stirred soln. of Cr complex, boiling gently, 30 min, concg. in high vac., dissolving in Et2O, addn. of (t-BuOCO)2O, addn. of 4-(dimethylamino)pyridine, 16 h; chromy. (SiO2, -20°C, Et2O/petroleum ether, 1:4 to 1:2); elem. anal.;