[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

Base Information

Chemical Name:[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]
CAS No.:906645-00-9
Molecular Formula:C₄₅H₃₅MnNO₃P₃Se₂
Molecular Weight:943.557
Hs Code.:

Synonyms:[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

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Chemical Property of [Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

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Technology Process of [Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

There total 2 articles about [Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 57693-96-6,65437-12-9,13682-00-3
{(PPh₃)manganese(carbonyl)4 bromide}

: potassium bis(diphenylselenophosphoryl)amide

: 906645-00-9
[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

Guidance literature:: In toluene; (N2); addn. of selenium compd. in toluene to soln. of manganese compd. in dry toluene, reflux for 1 h; filtration, evapn.;
DOI:10.1016/j.jorganchem.2006.03.027

Reference yield: 69.0%

: 765936-39-8
[Mn(CO)4(tetraphenyldiselenoimidophosphinato-κ2Se)]

: 603-35-0
triphenylphosphine

: 906645-00-9
[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

Guidance literature:: In toluene; (N2); addn. of soln. of phosphine deriv. in toluene to soln. of manganese compd. in dry toluene, reflux for 10 min; evapn., recrystn. (hexane) at 4°C, NMR;
DOI:10.1016/j.jorganchem.2006.03.027

Reference yield:

: 906645-00-9
[Mn(CO)3(triphenylphosphine)(tetraphenyldiselenoimidophosphinato-κ2Se)]

: 1313-13-9
manganese(IV) oxide

Guidance literature:: In dichloromethane; byproducts: Ph3PSe; keeping manganese compd. in CH2Cl2 soln. at room temp.;
DOI:10.1016/j.jorganchem.2006.03.027