C₁₆H₉Br₂F

Base Information

• Chemical Name: C₁₆H₉Br₂F
• CAS No.: 1227172-61-3
• Molecular Formula: C₁₆H₉Br₂F
• Molecular Weight: 380.054
• Mol file: 1227172-61-3.mol

Synonyms:C₁₆H₉Br₂F

Chemical Property of C₁₆H₉Br₂F

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₆H₉Br₂F

There total 1 articles about C₁₆H₉Br₂F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon tetrabromide (558-13-4) + 4-fluoro-2-(phenyl ethynyl)benzaldehyde (1189207-30-4) → C16H9Br2F (1227172-61-3)

Guidance literature:

With triethylamine; triphenylphosphine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1039/b926763h

Reference yield: 82.0%

C16H9Br2F (1227172-61-3) + phenylboronic acid (98-80-6) → 1-(diphenylmethylene)-6-fluoro-2-phenyl-1H-indene (1227172-72-6)

Guidance literature:

With potassium phosphate monohydrate; palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1039/b926763h

Reference yield: 75.0%

C16H9Br2F (1227172-61-3) + 4-methoxycarbonylphenylboronic acid (99768-12-4) → 2-(4-(methoxycarbonyl)phenyl)-1-((4-(methoxycarbonyl)phenyl)(phenyl)methylene)-6-fluoro-1H-indene

Guidance literature:

With potassium phosphate monohydrate; palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; stereoselective reaction; Inert atmosphere;

DOI:10.1039/b926763h

upstream raw materials:

carbon tetrabromide

4-fluoro-2-(phenyl ethynyl)benzaldehyde

Downstream raw materials:

1-(diphenylmethylene)-6-fluoro-2-phenyl-1H-indene

1-((4-fluoro-2-(phenylethynyl)phenyl)ethynyl)-1H-benzo[d]imidazole