bis(3-methoxyphenyl)(phenyl)phosphine oxide

Base Information

Chemical Name:bis(3-methoxyphenyl)(phenyl)phosphine oxide
CAS No.:216164-54-4
Molecular Formula:C₂₀H₁₉O₃P
Molecular Weight:338.343
Hs Code.:

Synonyms:bis(3-methoxyphenyl)(phenyl)phosphine oxide

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Chemical Property of bis(3-methoxyphenyl)(phenyl)phosphine oxide

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Technology Process of bis(3-methoxyphenyl)(phenyl)phosphine oxide

There total 7 articles about bis(3-methoxyphenyl)(phenyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2398-37-0
3-methoxyphenyl bromide

: 644-97-3
Dichlorophenylphosphine

: 216164-54-4
bis(3-methoxyphenyl)(phenyl)phosphine oxide

Guidance literature:: 3-methoxyphenyl bromide; With magnesium;

Dichlorophenylphosphine;

With water; dihydrogen peroxide; In tetrahydrofuran; Further stages.;
DOI:10.1039/a909495d

Reference yield: 98.0%

: 71360-01-5
ortho-methoxydiphenylphosphine oxide

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 216164-54-4
bis(3-methoxyphenyl)(phenyl)phosphine oxide

Guidance literature:: With copper(l) iodide; cesium fluoride; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.joc.6b01776

Reference yield: 38.0%

: 766-85-8
3-methoxy-1-iodobenzene

: 791-28-6
Triphenylphosphine oxide

: 95278-09-4
(3-methoxylphenyl)diphenylphosphine oxide

: 40331-46-2
tris(3-methoxyphenyl)phosphane oxide

: 216164-54-4
bis(3-methoxyphenyl)(phenyl)phosphine oxide

Guidance literature:: 3-methoxy-1-iodobenzene; With n-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 2h; Inert atmosphere; Schlenk technique;

Triphenylphosphine oxide; In diethyl ether; hexane; cyclohexane; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2015.12.043