Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)

Base Information

Chemical Name:Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)
CAS No.:795275-77-3
Molecular Formula:C10H19 N
Molecular Weight:153.26456
Hs Code.:
Mol file:795275-77-3.mol

Synonyms:Cyclohexanamine,3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)

Suppliers and Price of Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)

Chemical Property:

PSA：26.02000
LogP:3.02630

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI)

There total 2 articles about Cyclohexanamine, 3-methyl-2-(2-propenyl)-, (1R,2S,3R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 795275-76-2
2-[(1R,2S,3R)-2-allyl-3-methylcyclohexyl]-1H-isoindole-1,3(2H)-dione

: 795275-77-3
(1R,2S,3R)-2-allyl-3-methylcyclohexylamine

Guidance literature:: With 1-hexene; hydrazine hydrate; In ethanol; Heating;
DOI:10.1016/j.tet.2004.06.148

Reference yield:

: 795275-74-0
(3R)-2-allyl-3-methylcyclohexanone

: 795275-77-3
(1R,2S,3R)-2-allyl-3-methylcyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlH₄ / tetrahydrofuran / 3 h / -80 °C

1.2: 3.79 g / diethyl azodicarboxylate; PPh₃; (i-Pr₂)NEt / tetrahydrofuran / 3.5 h / 0 - 30 °C

2.1: hydrazine hydrate; 1-hexene / ethanol / Heating

With lithium aluminium tetrahydride; 1-hexene; hydrazine hydrate; In tetrahydrofuran; ethanol; 1.2: Mitsunobu reaction;
DOI:10.1016/j.tet.2004.06.148