Technology Process of 2-(cyclohepta-2,4,6-trienyl)-1-phenylethan-1-one (E)-O-pentafluorobenzoyloxime
There total 2 articles about 2-(cyclohepta-2,4,6-trienyl)-1-phenylethan-1-one (E)-O-pentafluorobenzoyloxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / pyridine; hydroxylamine hydrochloride / ethanol / 12 h / 60 °C
2: 95 percent / triethylamine / CH2Cl2 / 0.25 h / 0 °C
With
pyridine; hydroxylamine hydrochloride; triethylamine;
In
ethanol; dichloromethane;
DOI:10.1246/bcsj.77.785
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 68 percent / CH3COOH / methanol / 3 h / Heating
2: 95 percent / pyridine; hydroxylamine hydrochloride / ethanol / 12 h / 60 °C
3: 95 percent / triethylamine / CH2Cl2 / 0.25 h / 0 °C
With
pyridine; hydroxylamine hydrochloride; acetic acid; triethylamine;
In
methanol; ethanol; dichloromethane;
DOI:10.1246/bcsj.77.785
- Guidance literature:
-
2-(cyclohepta-2,4,6-trienyl)-1-phenylethan-1-one (E)-O-pentafluorobenzoyloxime;
With
tri-tert-butyl phosphine; 4 A molecular sieve; triethylamine;
bis(dibenzylideneacetone)-palladium(0);
In
N,N-dimethyl-formamide; toluene;
at 80 ℃;
for 0.5h;
With
manganese(IV) oxide;
In
dichloromethane;
for 2h;
Heating;
DOI:10.1246/bcsj.77.785
