C₁₈H₂₆Br₃IO₂

Base Information

Chemical Name:C₁₈H₂₆Br₃IO₂
CAS No.:1388632-06-1
Molecular Formula:C₁₈H₂₆Br₃IO₂
Molecular Weight:641.02
Hs Code.:

C<sub>18</sub>H<sub>26</sub>Br<sub>3</sub>IO<sub>2</sub>

Synonyms:C₁₈H₂₆Br₃IO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₆Br₃IO₂

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Technology Process of C₁₈H₂₆Br₃IO₂

There total 1 articles about C₁₈H₂₆Br₃IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 629-03-8
1 ,6-dibromohexane

: 216306-47-7
2-bromo-5-iodo-1,4-dihydroxybenzol

: 1388632-06-1
C₁₈H₂₆Br₃IO₂

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; at 75 ℃; for 72h;
DOI:10.1021/ja304986t

Reference yield: 54.0%

: 1074-61-9
(4-vinyl-phenyl)-methanol

: 1388632-06-1
C₁₈H₂₆Br₃IO₂

: 1388632-07-2
C₂₇H₃₅Br₃O₃

Guidance literature:: With tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine; In toluene; at 80 ℃; for 24h;
DOI:10.1021/ja304986t

Reference yield:

: 1388632-06-1
C₁₈H₂₆Br₃IO₂

: 1388632-09-4
C₆₆H₈₂I₄O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine / toluene / 24 h / 80 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 12 h / 100 °C / Inert atmosphere

3.1: tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine / toluene / 48 h / Inert atmosphere

3.2: Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributyl-amine; palladium diacetate; tris-(o-tolyl)phosphine; In toluene;
DOI:10.1021/ja304986t