benzyl 3-oxodecanoate

Base Information

Chemical Name:benzyl 3-oxodecanoate
CAS No.:66696-94-4
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:benzyl 3-oxodecanoate

Suppliers and Price of benzyl 3-oxodecanoate

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Chemical Property of benzyl 3-oxodecanoate

Chemical Property:

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Technology Process of benzyl 3-oxodecanoate

There total 5 articles about benzyl 3-oxodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2033-24-1
cycl-isopropylidene malonate

: 111-64-8
n-octanoic acid chloride

: 100-51-6,185532-71-2
benzyl alcohol

: 66696-94-4
benzyl 3-oxodecanoate

Guidance literature:: cycl-isopropylidene malonate; With pyridine; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;

n-octanoic acid chloride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

benzyl alcohol; for 3h; Reflux; Inert atmosphere;
DOI:10.1021/jacs.7b00427

Reference yield: 90.0%

: 103576-44-9
2,2-dimethyl-5-octanoyl-1,3-dioxane-4,6-dione

: 100-51-6,185532-71-2
benzyl alcohol

: 66696-94-4
benzyl 3-oxodecanoate

Guidance literature:: In toluene; at 80 ℃; for 8.5h;
DOI:10.1021/acs.jnatprod.0c00441

Reference yield:

: 124-07-2
Octanoic acid

: 66696-94-4
benzyl 3-oxodecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C

2: dmap / dichloromethane / 3 h / 20 °C

3: toluene / 8.5 h / 80 °C

With dmap; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1021/acs.jnatprod.0c00441