Decanoic acid, 3-hydroxy-, phenylmethyl ester

Base Information

Chemical Name:Decanoic acid, 3-hydroxy-, phenylmethyl ester
CAS No.:132016-02-5
Molecular Formula:C17H26O3
Molecular Weight:278.392
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Decanoic acid, 3-hydroxy-, phenylmethyl ester

Chemical Property:

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Technology Process of Decanoic acid, 3-hydroxy-, phenylmethyl ester

There total 6 articles about Decanoic acid, 3-hydroxy-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 66696-94-4
benzyl 3-oxodecanoate

: 132016-02-5
benzyl (±)-3-hydroxydecanoate

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; water; at 20 ℃; for 1.25h; pH=Ca. 3; Inert atmosphere;
DOI:10.1021/jacs.7b00427

Reference yield: 64.0%

: 5561-87-5,19525-80-5,19526-23-9,33044-91-6,14292-26-3
3-hydroxydecanoic acid

: 100-39-0
benzyl bromide

: 132016-02-5
benzyl (±)-3-hydroxydecanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.bioorg.2019.03.023

Reference yield:

: 111-64-8
n-octanoic acid chloride

: 132016-02-5
benzyl (±)-3-hydroxydecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

1.3: 3 h / Reflux; Inert atmosphere

2.1: sodium cyanoborohydride; hydrogenchloride / tetrahydrofuran; water / 1.25 h / 20 °C / pH Ca_. 3 / Inert atmosphere

With pyridine; hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; water;
DOI:10.1021/jacs.7b00427