C₃₆H₄₃Cl₅N₂O₈Si

Base Information

Chemical Name:C₃₆H₄₃Cl₅N₂O₈Si
CAS No.:1380572-72-4
Molecular Formula:C₃₆H₄₃Cl₅N₂O₈Si
Molecular Weight:837.097
Hs Code.:

C<sub>36</sub>H<sub>43</sub>Cl<sub>5</sub>N<sub>2</sub>O<sub>8</sub>Si

Synonyms:C₃₆H₄₃Cl₅N₂O₈Si

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Chemical Property of C₃₆H₄₃Cl₅N₂O₈Si

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Technology Process of C₃₆H₄₃Cl₅N₂O₈Si

There total 5 articles about C₃₆H₄₃Cl₅N₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

: 1380572-72-4
C₃₆H₄₃Cl₅N₂O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

3: 1H-imidazole / dichloromethane / 4 h

4: N-Bromosuccinimide; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / Darkness

With 1H-imidazole; N-Bromosuccinimide; sulfuryl dichloride; boron trifluoride diethyl etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-64-4
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methanone

: 1380572-72-4
C₃₆H₄₃Cl₅N₂O₈Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 3 h / 0 °C

3.1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

5.1: 1H-imidazole / dichloromethane / 4 h

6.1: N-Bromosuccinimide; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / Darkness

With 1H-imidazole; N-Bromosuccinimide; lithium borohydride; sulfuryl dichloride; boron trifluoride diethyl etherate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 33719-74-3
3,5-dichloroanisole

: 1380572-72-4
C₃₆H₄₃Cl₅N₂O₈Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / nitrobenzene / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

3.2: 3 h / 0 °C

4.1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

6.1: 1H-imidazole / dichloromethane / 4 h

7.1: N-Bromosuccinimide; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / Darkness

With 1H-imidazole; aluminum (III) chloride; N-Bromosuccinimide; lithium borohydride; sulfuryl dichloride; boron trifluoride diethyl etherate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; nitrobenzene; N,N-dimethyl-formamide; acetonitrile; mineral oil; 1.1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2012.03.121