((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

Base Information

Chemical Name:((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride
CAS No.:1380572-67-7
Molecular Formula:C₁₅H₁₀Cl₆O₂
Molecular Weight:434.961
Hs Code.:

Synonyms:((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

Chemical Property:

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Technology Process of ((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

There total 4 articles about ((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

: 1380572-67-7
((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

Guidance literature:: With sulfuryl dichloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-64-4
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methanone

: 1380572-67-7
((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 3 h / 0 °C

3.1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

With lithium borohydride; sulfuryl dichloride; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 33719-74-3
3,5-dichloroanisole

: 1380572-67-7
((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / nitrobenzene / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

3.2: 3 h / 0 °C

4.1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

With aluminum (III) chloride; lithium borohydride; sulfuryl dichloride; sodium hydride; In tetrahydrofuran; dichloromethane; nitrobenzene; mineral oil; 1.1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2012.03.121