(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

Base Information

Chemical Name:(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide
CAS No.:1380572-66-6
Molecular Formula:C₁₆H₁₃Cl₅O₂S
Molecular Weight:446.609
Hs Code.:

Synonyms:(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

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Chemical Property of (((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

Chemical Property:

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Technology Process of (((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

There total 3 articles about (((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2373-51-5
chloro-methylsulfanyl-methane

: 1380572-65-5
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methanol

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

Guidance literature:: (2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃;

chloro-methylsulfanyl-methane; In tetrahydrofuran; mineral oil; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 33719-74-3
3,5-dichloroanisole

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / nitrobenzene / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

3.2: 3 h / 0 °C

With aluminum (III) chloride; lithium borohydride; sodium hydride; In tetrahydrofuran; nitrobenzene; mineral oil; 1.1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / nitrobenzene / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

3.2: 3 h / 0 °C

With aluminum (III) chloride; lithium borohydride; sodium hydride; In tetrahydrofuran; nitrobenzene; mineral oil; 1.1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2012.03.121