N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Base Information

Chemical Name:N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>
CAS No.:174709-61-6
Molecular Formula:C₂₄H₃₆N₂O₁₀S₄
Molecular Weight:640.821
Hs Code.:

Synonyms:N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

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Chemical Property of N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

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Technology Process of N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

There total 5 articles about N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124-63-0
methanesulfonyl chloride

: 174709-60-5
N,N'-bis(p-toluenesulfonyl)-N,N'-bis(3-hydroxypropyl)ethylenediamine

: 174709-61-6
N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo951499w

Reference yield:

: 32705-91-2
ethylenediamine-N,N'-di-3-propionic acid dihydrochloride salt

: 174709-61-6
N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / sodium hydroxide / dioxane; H₂O

2: 96 percent / BH₃*THF / tetrahydrofuran / Ambient temperature

3: 90 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With sodium hydroxide; borane-THF; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo951499w

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 174709-61-6
N,N'-ethylenebis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / sodium hydroxide / dioxane; H₂O

2: 96 percent / BH₃*THF / tetrahydrofuran / Ambient temperature

3: 90 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With sodium hydroxide; borane-THF; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo951499w