N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

Base Information

Chemical Name:N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide
CAS No.:1293408-35-1
Molecular Formula:C₁₃H₁₉NO₆
Molecular Weight:285.297
Hs Code.:

Synonyms:N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

Chemical Property:

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Technology Process of N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

There total 5 articles about N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₆N₂O₅

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1293408-35-1
N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

Guidance literature:: With triethylamine; In acetonitrile; at 40 ℃; for 20h;
DOI:10.1016/j.bmcl.2011.01.124

Reference yield:

: 17609-89-1
C₁₃H₁₈O₄

: 1293408-35-1
N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; ozone / methanol; chloroform / -15 °C

2: urea hydrogen peroxide adduct; sodium hydroxide / methanol; water / 1.5 h / Reflux

3: acetonitrile / 0.33 h / 20 °C

4: triethylamine / acetonitrile / 20 h / 40 °C

With pyridine; urea hydrogen peroxide adduct; ozone; triethylamine; sodium hydroxide; In methanol; chloroform; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.124

Reference yield:

: 15361-99-6
1,2,3,4-Tetramethoxy-5-(2-propenyl)benzene

: 1293408-35-1
N-methoxy-N-methyl-2,3,4,5-tetramethoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C / Neat (no solvent)

2: pyridine; ozone / methanol; chloroform / -15 °C

3: urea hydrogen peroxide adduct; sodium hydroxide / methanol; water / 1.5 h / Reflux

4: acetonitrile / 0.33 h / 20 °C

5: triethylamine / acetonitrile / 20 h / 40 °C

With pyridine; tetrabutylammomium bromide; urea hydrogen peroxide adduct; ozone; triethylamine; potassium hydroxide; sodium hydroxide; In methanol; chloroform; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.124