(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

Base Information

Chemical Name:(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester
CAS No.:74510-46-6
Molecular Formula:C₁₁H₁₃BrClNO₃
Molecular Weight:322.586
Hs Code.:

Synonyms:(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

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Chemical Property of (5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

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Technology Process of (5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

There total 12 articles about (5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74510-45-5
(2-Chloro-3-methoxy-5-methyl-phenyl)-methyl-carbamic acid methyl ester

: 74510-46-6
(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 4h; Heating;

Reference yield:

: 2835-98-5
2-Hydroxy-4-methylanilin

: 74510-46-6
(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 12 steps

1: sodium bicarbonate / H₂O; CH₂Cl₂ / Ambient temperature

2: potassium carbonate / acetone / Heating

3: 1.) n-butyllithium / 1.) THF, rt, 6 h; 2.) -70 deg C

4: 95 percent / aq. hydrochloric acid / 16 h / Heating

5: sodium nitrite / aq. HCl / 0 °C

6: cuprous chloride / aq. HCl / 48 h / 60 °C

7: triethylamine / acetone

8: sodium azide / H₂O / 0 °C

9: benzene / 0.5 h / 60 °C

10: 1 h / 80 °C

11: sodium hydride / tetrahydrofuran / 0 °C

12: 80 percent / benzoyl peroxide, N-bromosuccinimide / CCl₄ / 4 h / Heating

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; sodium azide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triethylamine; copper(l) chloride; sodium nitrite; dibenzoyl peroxide; In tetrahydrofuran; hydrogenchloride; tetrachloromethane; dichloromethane; water; acetone; benzene;

Reference yield:

: 98922-98-6
2'-hydroxy-2,2,4'-trimethylpropionanilide

: 74510-46-6
(5-Bromomethyl-2-chloro-3-methoxy-phenyl)-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: potassium carbonate / acetone / Heating

2: 1.) n-butyllithium / 1.) THF, rt, 6 h; 2.) -70 deg C

3: 95 percent / aq. hydrochloric acid / 16 h / Heating

4: sodium nitrite / aq. HCl / 0 °C

5: cuprous chloride / aq. HCl / 48 h / 60 °C

6: triethylamine / acetone

7: sodium azide / H₂O / 0 °C

8: benzene / 0.5 h / 60 °C

9: 1 h / 80 °C

10: sodium hydride / tetrahydrofuran / 0 °C

11: 80 percent / benzoyl peroxide, N-bromosuccinimide / CCl₄ / 4 h / Heating

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; sodium azide; sodium hydride; potassium carbonate; triethylamine; copper(l) chloride; sodium nitrite; dibenzoyl peroxide; In tetrahydrofuran; hydrogenchloride; tetrachloromethane; water; acetone; benzene;