C₁₇H₁₃BrF₄N₂O₃

Base Information

Chemical Name:C₁₇H₁₃BrF₄N₂O₃
CAS No.:1416733-45-3
Molecular Formula:C₁₇H₁₃BrF₄N₂O₃
Molecular Weight:449.199
Hs Code.:

C<sub>17</sub>H<sub>13</sub>BrF<sub>4</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₇H₁₃BrF₄N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₃BrF₄N₂O₃

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Technology Process of C₁₇H₁₃BrF₄N₂O₃

There total 7 articles about C₁₇H₁₃BrF₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1416733-44-2
C₁₇H₁₅BrF₄N₂O₃

: 1416733-45-3
C₁₇H₁₃BrF₄N₂O₃

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 624-28-2
2,5-dibromopyridine

: 1416733-45-3
C₁₇H₁₃BrF₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper / dimethyl sulfoxide / 1 h / 20 °C

1.2: 15 h / 20 °C

2.1: n-butyllithium / hexane; diethyl ether / -70 - 20 °C

3.1: zinc / tetrahydrofuran / 0.5 h / 20 °C

3.2: 0 - 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

5.1: ammonia / N,N-dimethyl-formamide; water / 3 h / 60 °C

6.1: ethanol / 20 - 80 °C

7.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With n-butyllithium; ammonia; copper; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 294181-95-6
2-(5-bromopyridine-2-yl)-2,2-difluoroacetic acid ethyl ester

: 1416733-45-3
C₁₇H₁₃BrF₄N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; diethyl ether / -70 - 20 °C

2.1: zinc / tetrahydrofuran / 0.5 h / 20 °C

2.2: 0 - 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

4.1: ammonia / N,N-dimethyl-formamide; water / 3 h / 60 °C

5.1: ethanol / 20 - 80 °C

6.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With n-butyllithium; ammonia; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;