2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

Base Information

Chemical Name:2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate
CAS No.:862672-94-4
Molecular Formula:C₁₅H₁₆O₄S
Molecular Weight:292.356
Hs Code.:

Synonyms:2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

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Chemical Property of 2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

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Technology Process of 2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

There total 3 articles about 2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 862672-84-2
2-[(E)-butadienesulfonyl]-1-phenylethanol

: 79-10-7
acrylic acid

: 862672-94-4
2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

Guidance literature:: acrylic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 3h;

2-[(E)-butadienesulfonyl]-1-phenylethanol; With dmap; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/ol050930t

Reference yield:

: 862672-80-8
2-[(Z)-butadienesulfonyl]-1-phenylethanol

: 862672-94-4
2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4.29 g / DMAP / CH₂Cl₂ / 48 h / 20 °C

2.1: DCC / CH₂Cl₂ / 3 h

2.2: 81 percent / DMAP / CH₂Cl₂ / 15 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ol050930t

Reference yield:

: 862672-76-2
2-[(Z)-butadienesulfonyl]-1-phenylethanone

: 862672-94-4
2-[(E)-butadienesulfonyl]-1-phenylethyl acrylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / NaBH₄ / methanol; H₂O / 1.25 h / -5 °C

2.1: 4.29 g / DMAP / CH₂Cl₂ / 48 h / 20 °C

3.1: DCC / CH₂Cl₂ / 3 h

3.2: 81 percent / DMAP / CH₂Cl₂ / 15 h / 20 °C

With dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ol050930t