Technology Process of N,O-di(phenoxycarbonyl)-5-chlorooxindole
There total 5 articles about N,O-di(phenoxycarbonyl)-5-chlorooxindole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: naphthalene radical anion sodium salt / 1,2-dimethoxyethane / -78 - 0.18 °C
2: triethylamine / tetrahydrofuran / 1 h / 0 °C
With
naphthalene radical anion sodium salt; triethylamine;
In
tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1055/s-0035-1562619
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper diacetate; potassium phosphate / N,N-dimethyl-formamide / 18 h / 30 - 55 °C / Inert atmosphere
2: methanol; water / 4 h / 70 °C
3: oxone / water; acetone / 2 h
4: naphthalene radical anion sodium salt / 1,2-dimethoxyethane / -78 - 0.18 °C
5: triethylamine / tetrahydrofuran / 1 h / 0 °C
With
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; copper(l) iodide; oxone; copper diacetate; naphthalene radical anion sodium salt; triethylamine;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1055/s-0035-1562619
