(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide
CAS No.:1448295-59-7
Molecular Formula:C₃₀H₃₈N₂O₂S
Molecular Weight:490.71
Hs Code.:

Synonyms:(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

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Chemical Property of (E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

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Technology Process of (E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

There total 3 articles about (E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 100-39-0
benzyl bromide

: (E)-2,4,6-triisopropyl-N'-(1-phenylethylidene)benzenesulfonohydrazide

: 1448295-59-7
(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Guidance literature:: (E)-2,4,6-triisopropyl-N'-(1-phenylethylidene)benzenesulfonohydrazide; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

benzyl bromide; In tetrahydrofuran; at -78 ℃; for 1.5h;
DOI:10.1021/ol401637n

Reference yield:

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 1448295-59-7
(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine / tetrahydrofuran / 3 h / -10 - 0 °C

2.1: hydrogenchloride / methanol / 3 h / 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

3.2: 1.5 h / -78 °C

With hydrogenchloride; n-butyllithium; hydrazine; In tetrahydrofuran; methanol;
DOI:10.1021/ol401637n

Reference yield:

: 39085-59-1
trisylhydrazine

: 1448295-59-7
(E)-N'-(1,3-diphenylpropylidene)-2,4,6-triisopropylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / methanol / 3 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 1.5 h / -78 °C

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; methanol;
DOI:10.1021/ol401637n