C₁₆H₁₇BrOS

Base Information

• Chemical Name: C₁₆H₁₇BrOS
• CAS No.: 1554261-67-4
• Molecular Formula: C₁₆H₁₇BrOS
• Molecular Weight: 337.28
• Mol file: 1554261-67-4.mol

Synonyms:C₁₆H₁₇BrOS

Chemical Property of C₁₆H₁₇BrOS

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₆H₁₇BrOS

There total 3 articles about C₁₆H₁₇BrOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + ethanol (64-17-5) + 4-bromobenzenesulfonyl chloride (98-58-8) → C16H17BrOS (1554261-67-4)

Guidance literature:

With hydrogen bromide; tetra-(n-butyl)ammonium iodide; In water; ethyl acetate; at 80 ℃; for 15h; Schlenk technique;

DOI:10.1055/s-0035-1561667

Reference yield: 74.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-bromophenylsulfonyl hydrazide (2297-64-5) + ethanol (64-17-5) → C16H17BrOS (1554261-67-4)

Guidance literature:

With iodine; In 1,2-dichloro-ethane; at 70 ℃; for 16h; regioselective reaction;

DOI:10.1039/c3cc48961b

Reference yield: 72.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + ethanol (64-17-5) + sodium 4-bromobenzenesulfinate (34176-08-4) → C16H17BrOS (1554261-67-4)

Guidance literature:

With iodine; triphenylphosphine; In toluene; at 75 ℃; for 24h;

DOI:10.1039/c6ob00646a

upstream raw materials:

styrene

p-bromophenylsulfonyl hydrazide

ethanol

sodium 4-bromobenzenesulfinate