(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

Base Information

Chemical Name:(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide
CAS No.:733000-56-1
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

Chemical Property:

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Technology Process of (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

There total 1 articles about (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 733000-55-0
(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid ethyl ester

: 733000-56-1
(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

Guidance literature:: With isopropylmagnesium chloride; In tetrahydrofuran; at -20 - -10 ℃; for 6h;
DOI:10.1002/ejoc.200400047

Reference yield: 85.0%

: 3314-49-6
octyllithium

: 733000-56-1
(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

: 733000-57-2
(S)-4-((R)-2-Benzyloxy-1-hydroxy-ethyl)-tridec-1-en-5-one

Guidance literature:: In tetrahydrofuran; diethyl ether; at -10 ℃; for 5h;
DOI:10.1002/ejoc.200400047

Reference yield:

: 733000-56-1
(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-pent-4-enoic acid methoxy-methyl-amide

: (2R,3R)-3-Allyl-1-benzyloxy-dodecane-2,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetrahydrofuran; diethyl ether / 5 h / -10 °C

2: 94 percent / tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 21 h / -20 °C

With tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; diethyl ether; acetic acid; acetonitrile;
DOI:10.1002/ejoc.200400047