Pt(C_.ident.-3-thienyl)2(dppe)

Base Information

Chemical Name:Pt(C_.ident.-3-thienyl)2(dppe)
CAS No.:878379-17-0
Molecular Formula:C₃₈H₃₀P₂PtS₂
Molecular Weight:807.816
Hs Code.:

Pt(C<sub>.</sub>ident.-3-thienyl)2(dppe)

Synonyms:Pt(C_.ident.-3-thienyl)2(dppe)

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Chemical Property of Pt(C_.ident.-3-thienyl)2(dppe)

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Technology Process of Pt(C_.ident.-3-thienyl)2(dppe)

There total 1 articles about Pt(C_.ident.-3-thienyl)2(dppe) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67237-53-0
3-ethynylthiophene

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 878379-17-0
Pt(C_.ident.-3-thienyl)2(dppe)

Guidance literature:: With NH(CH₂CH₃)2; CuCl; In dichloromethane; diethylamine; addn. of alkyne and CuCl to a soln. of platinum complex in diethylamine and CH2Cl2 (1:1), reflux overnight; evapn., dissolving in CH2Cl2, washing with H2O, drying org. layer over Na2SO4, filtration, concn., addn. of hexane, standing at room temp. for several minutes; elem. anal.;
DOI:10.1021/om050748w

Reference yield: 54.0%

: 84896-12-8,168038-94-6
Ru₃(CO)11(acetonitrile)

: 75-09-2
dichloromethane

: 878379-17-0
Pt(C_.ident.-3-thienyl)2(dppe)

: [PtRu3(μ4-η1:η1:η1:η4:η4-C4H2SCCC(H)C-3-thienyl)(μ-CO)2(CO)6(dppe)]*0.5CH2Cl2

Guidance literature:: In toluene; addn. of ruthenium cluster to a soln. of platinum complex in toluene, reflux for 45 min, cooling; evapn., thin layer chromy. (SiO2, CH2Cl2), recrystn. (toluene/CH2Cl2); elem. anal.;
DOI:10.1021/om050748w

Reference yield: 15.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 878379-17-0
Pt(C_.ident.-3-thienyl)2(dppe)

: 108-88-3,15644-74-3,16713-13-6
toluene

: [FePt(μ2-η1:η1:η4-(C4(3-thienyl)2-CO)-CO)(CO)3(dppe)]

: [FePt(μ2-η1:η1:η2-(3-thienyl)CCCC(3-thienyl)-CO)(CO)(CO)2(dppe)]*0.5toluene

Guidance literature:: In toluene; addn. of iron complex to a soln. of platinum complex in toluene, reflux for 45 min, cooling; evapn., thin layer chromy. (SiO2), recrystn. (toluene); elem. anal.;
DOI:10.1021/om050748w