(4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate

Base Information Edit

Chemical Name:(4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate
CAS No.:1206732-30-0
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:
Mol file:1206732-30-0.mol

Synonyms:(4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate

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Chemical Property of (4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate Edit

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Technology Process of (4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate

There total 2 articles about (4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 105-13-5
4-Methoxybenzyl alcohol

: 154568-28-2
(R,R)-2-[trans-2-(ethoxycarbonyl)vinyl]-3-methyloxirane

: 1206732-30-0
(4R,5R,E)-ethyl 5-hydroxy-4-(4-methoxybenzyloxy)hex-2-enoate

Guidance literature:: 4-Methoxybenzyl alcohol; With triphenylborane; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

(R,R)-2-[trans-2-(ethoxycarbonyl)vinyl]-3-methyloxirane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.12.125