(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2

Base Information

• Chemical Name: (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2
• CAS No.: 255713-45-2
• Molecular Formula: C₃₅H₅₉N₃Si₂Zn
• Molecular Weight: 643.435

Synonyms:(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2

Chemical Property of (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2

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Technology Process of (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2

There total 3 articles about (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

bis(bis(trimethylsilyl)amido)zinc(II) + 2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene (289618-59-3) → (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe3)2 (255713-45-2)

Guidance literature:

In toluene; (N2); addn. of a soln. of ligand in toluene to a soln. of zinc compd. intoluene at room temp., stirring for 6 d at 80°C; evapn., drying in vac., crystn. (toluene, -30°C);

DOI:10.1021/ja003850n

Reference yield: 70.0%

bis(bis(trimethylsilyl)amido)zinc(II) + 2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene → (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe3)2 (255713-45-2)

Guidance literature:

In toluene; at 80 ℃; for 18h;

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) + acetylacetone (123-54-6,81235-32-7) → (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe3)2 (255713-45-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 48 h / Reflux

2: toluene / 18 h / 80 °C

With hydrogenchloride; In methanol; water; toluene;

upstream raw materials:

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene

2,6-diisopropylbenzenamine

acetylacetone

Downstream raw materials:

[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

(CH(CMeNC₆H₃-2,6-(i)Pr₂)2)ZnOSiPh₃(THF)

rac-(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOCH(Me)CO₂Me

[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-penteneato)ZnOAc]

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