[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

Base Information

Chemical Name:[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2
CAS No.:215808-46-1
Molecular Formula:C₆₂H₈₈N₄O₄Zn₂
Molecular Weight:1084.19
Hs Code.:

Synonyms:[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

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Chemical Property of [(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

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Technology Process of [(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

There total 4 articles about [(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 215808-47-2
(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc

: 64-19-7,77671-22-8
acetic acid

: 215808-46-1
[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

Guidance literature:: In hexane; (N2); AcOH added dropwise to a soln. of Zn complex at 0°C, stirred overnight allowing gradual warming to room temp.; evapn. (vac.), crystn. (CH2Cl2, -20°C);
DOI:10.1016/S0022-328X(03)00544-8

Reference yield: 63.0%

: 557-34-6
zinc diacetate

: 289618-59-3
2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene

: 215808-46-1
[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; (N2); addn. of a soln. of BuLi in hexane to a soln. of ligand in THF at 0°C, stirring for 5 min at 0°C, addn. to a soln. of zinc acetate in THF, stirring overnight at room temp.; filtration, drying in vac., recrystn. (CH2Cl2, -20°C);
DOI:10.1021/ja003850n

Reference yield: 34.0%

: 255713-45-2
(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnN(SiMe₃)2

: 64-19-7,77671-22-8
acetic acid

: 215808-46-1
[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

Guidance literature:: In toluene; (N2); addn. of glacial acetic acid to a soln. of zinc complex in toluene, stirring for 18 h at 20°C; evapn., recrystn. (CH2Cl2);
DOI:10.1021/ja003850n