1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

Base Information

Chemical Name:1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane
CAS No.:1375488-87-1
Molecular Formula:C₃₉H₃₈N₆O₆S₂
Molecular Weight:750.899
Hs Code.:

Synonyms:1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

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Chemical Property of 1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

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Technology Process of 1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

There total 2 articles about 1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1375488-86-0
1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

: 105-36-2
ethyl bromoacetate

: 1375488-87-1
1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

Guidance literature:: With potassium hydroxide; In methanol; at 0 - 20 ℃;
DOI:10.1002/jhet.729

Reference yield:

: 62-53-3
aniline

: 1375488-87-1
1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / Heating

2: potassium hydroxide / methanol / Reflux

3: potassium hydroxide / methanol / 0 - 20 °C

With potassium hydroxide; In methanol;
DOI:10.1002/jhet.729

Reference yield: 46.0%

: 1375488-87-1
1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

: 1375488-88-2
1,9-dibenzena-2,8-(3,5)-1,2,4-triazola-10,14-dioxa-3,7-dithia-2⁽⁴⁾,8⁽⁴⁾-diphenyl-12-oxocyclotetradecaphane

Guidance literature:: 1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane; With sodium methylate; In methanol; at 20 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; In methanol; water; Cooling with ice; Inert atmosphere;
DOI:10.1002/jhet.729