1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

Base Information

Chemical Name:1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane
CAS No.:1375488-86-0
Molecular Formula:C₃₁H₂₆N₆O₂S₂
Molecular Weight:578.718
Hs Code.:

Synonyms:1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

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Chemical Property of 1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

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Technology Process of 1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

There total 1 articles about 1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81518-26-5
4-phenyl-5-(2'-hydroxyphenyl)-3-mercapto-1,2,4-triazole

: 109-64-8
1,3-dibromo-propane

: 1375488-86-0
1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

Guidance literature:: With potassium hydroxide; In methanol; Reflux;
DOI:10.1002/jhet.729

Reference yield: 82.0%

: 1375488-86-0
1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

: 105-36-2
ethyl bromoacetate

: 1375488-87-1
1,3-bis[{5-(4-phenyl-2'-carbethoxyphenyl)-1,2,4-triazol-3-yl}mercapto]propane

Guidance literature:: With potassium hydroxide; In methanol; at 0 - 20 ℃;
DOI:10.1002/jhet.729

Reference yield:

: 1375488-86-0
1,3-bis[4-phenyl-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercaptopropane

: 1375488-88-2
1,9-dibenzena-2,8-(3,5)-1,2,4-triazola-10,14-dioxa-3,7-dithia-2⁽⁴⁾,8⁽⁴⁾-diphenyl-12-oxocyclotetradecaphane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol / 0 - 20 °C

2.1: sodium methylate / methanol / 6 h / 20 °C / Inert atmosphere

2.2: Cooling with ice; Inert atmosphere

With sodium methylate; potassium hydroxide; In methanol; 2.1: Dieckmann reaction;
DOI:10.1002/jhet.729