Technology Process of Methyl 4-(tert-Butyldiphenylsiloxy)-5-methyl-hexa-2(E),5-dienoate
There total 6 articles about Methyl 4-(tert-Butyldiphenylsiloxy)-5-methyl-hexa-2(E),5-dienoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / periodic acid dihydrate / diethyl ether / 4 h / Ambient temperature
2: 1) NaH / 1) benzene, room temp., 30 min., 2) benzene, 30 min.
With
sodium hydride; periodic acid;
In
diethyl ether;
DOI:10.1248/cpb.38.1451
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / trifluoroacetic acid / methanol / 2 h / 70 °C
2: 94 percent / periodic acid dihydrate / diethyl ether / 4 h / Ambient temperature
3: 1) NaH / 1) benzene, room temp., 30 min., 2) benzene, 30 min.
With
sodium hydride; periodic acid; trifluoroacetic acid;
In
methanol; diethyl ether;
DOI:10.1248/cpb.38.1451
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91 percent / SOCl2, pyridine / 1 h / Ambient temperature
2: 91 percent / trifluoroacetic acid / methanol / 2 h / 70 °C
3: 94 percent / periodic acid dihydrate / diethyl ether / 4 h / Ambient temperature
4: 1) NaH / 1) benzene, room temp., 30 min., 2) benzene, 30 min.
With
pyridine; thionyl chloride; sodium hydride; periodic acid; trifluoroacetic acid;
In
methanol; diethyl ether;
DOI:10.1248/cpb.38.1451