C₄₉H₅₆FN₃O₇Si

Base Information

Chemical Name:C₄₉H₅₆FN₃O₇Si
CAS No.:1253799-30-2
Molecular Formula:C₄₉H₅₆FN₃O₇Si
Molecular Weight:846.083
Hs Code.:

C<sub>49</sub>H<sub>56</sub>FN<sub>3</sub>O<sub>7</sub>Si

Synonyms:C₄₉H₅₆FN₃O₇Si

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Chemical Property of C₄₉H₅₆FN₃O₇Si

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Technology Process of C₄₉H₅₆FN₃O₇Si

There total 5 articles about C₄₉H₅₆FN₃O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1253799-29-9
phenyl 2-(benzyloxy)-3-(dibenzylamino)-5-fluoro-6-methylbenzoate

: 1253799-28-8
C₂₇H₃₆N₂O₅Si

: 1253799-30-2
C₄₉H₅₆FN₃O₇Si

Guidance literature:: phenyl 2-(benzyloxy)-3-(dibenzylamino)-5-fluoro-6-methylbenzoate; With N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

C₂₇H₃₆N₂O₅Si; With lithium hexamethyldisilazane; In tetrahydrofuran; hexane; at -78 - -15 ℃; for 1.33333h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; water; Inert atmosphere;

Reference yield:

: 856906-36-0
C₂₀H₂₀N₂O₅

: 1253799-30-2
C₄₉H₅₆FN₃O₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.58 h / 0 - 23 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.78 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: pyridine; N-chloro-succinimide / dichloromethane / 5.5 h / 0 - 23 °C / Inert atmosphere

4.1: copper(l) iodide / diethyl ether / -78 °C / Inert atmosphere

5.1: N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

5.2: 1.33 h / -78 - -15 °C / Inert atmosphere

5.3: Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-chloro-succinimide; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 1253798-65-0
C₂₀H₂₀N₂O₅

: 1253799-30-2
C₄₉H₅₆FN₃O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium dihydrogenphosphate / tetrahydrofuran; methanol; water / 52 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 0.58 h / 0 - 23 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.78 h / 0 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: pyridine; N-chloro-succinimide / dichloromethane / 5.5 h / 0 - 23 °C / Inert atmosphere

5.1: copper(l) iodide / diethyl ether / -78 °C / Inert atmosphere

6.1: N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

6.2: 1.33 h / -78 - -15 °C / Inert atmosphere

6.3: Inert atmosphere

With pyridine; 2,6-dimethylpyridine; sodium dihydrogenphosphate; N-chloro-succinimide; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;