2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

Base Information

Chemical Name:2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide
CAS No.:175353-08-9
Molecular Formula:C₄₆H₅₀N₄O₈
Molecular Weight:786.925
Hs Code.:

Synonyms:2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

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Technology Process of 2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

There total 3 articles about 2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131933-37-4
2,3-bis(benzyloxy)-terephthalic acid

: 175353-08-9
2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / N,N-dicyclohexylcarbodiimide / dimethylformamide / Ambient temperature

2: triethylamine / dioxane / 40 h / Ambient temperature

3: aq. Na₂CO₃ / dioxane; ethyl acetate / 3 h / Ambient temperature

With sodium carbonate; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 131851-95-1
2,3-dibenzyloxyterephthalic acid N-hydroxysuccinimide diester

: 175353-08-9
2,3-dibenzyloxyterephthalic acid bis<(N-acetyl-N-benzyloxy)-1,3-diaminopropyl>amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dioxane / 40 h / Ambient temperature

2: aq. Na₂CO₃ / dioxane; ethyl acetate / 3 h / Ambient temperature

With sodium carbonate; triethylamine; In 1,4-dioxane; ethyl acetate;