C₃₁H₂₁Cl

Base Information

• Chemical Name: C₃₁H₂₁Cl
• CAS No.: 1221237-90-6
• Molecular Formula: C₃₁H₂₁Cl
• Molecular Weight: 428.961
• Mol file: 1221237-90-6.mol

Synonyms:C₃₁H₂₁Cl

Chemical Property of C₃₁H₂₁Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₁H₂₁Cl

There total 1 articles about C₃₁H₂₁Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-Chlorophenylboronic acid (1679-18-1) + 2-bromo-9,9-diphenyl-9H-fluorene (474918-32-6) → C31H21Cl (1221237-90-6)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; for 5h; Heating;

Reference yield: 65.0%

C31H21Cl (1221237-90-6) + aniline (62-53-3) → C37H27N (1221237-91-7)

Guidance literature:

With sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; for 1h; Inert atmosphere; Heating;

Reference yield:

C31H21Cl (1221237-90-6) → C62H44N2 (1221237-18-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 1 h / Inert atmosphere; Heating

2: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / xylene / 1 h / Inert atmosphere; Heating

With sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; xylene;

upstream raw materials:

4-Chlorophenylboronic acid

2-bromo-9,9-diphenyl-9H-fluorene

Downstream raw materials:

C₃₇H₂₇N

C₆₂H₄₄N₂

Refernces