3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate

Base Information

• Chemical Name: 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate
• CAS No.: 1123661-10-8
• Molecular Formula: C₂HF₃O₂*C₁₄H₁₈N₂O₂
• Molecular Weight: 360.333

Synonyms:3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate

Chemical Property of 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate

Chemical Property:

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Technology Process of 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate

There total 3 articles about 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-benzyl-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-benzyloxybenzamide (1123661-18-6) + trifluoroacetic acid (76-05-1) → 3-exo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide + 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate (1123661-10-8)

Guidance literature:

With hydrogen; palladium hydroxide on carbon; In methanol; under 1551.49 Torr;

Reference yield:

3-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-hydroxybenzamide trifluoroacetate (1123661-07-3) + 3-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-benzyloxybenzamide trifluoroacetate (1123661-03-9) → 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate (1123661-10-8)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; Product distribution / selectivity;

Reference yield:

3-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-benzyloxybenzamide trifluoroacetate (1123661-03-9) → 3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide trifluoroacetate (1123661-10-8)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; Product distribution / selectivity;

upstream raw materials:

8-benzyl-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-benzyloxybenzamide

trifluoroacetic acid

3-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-benzyloxybenzamide trifluoroacetate

3-(8-azabicyclo[3.2.1]oct-2-en-3-yl)-2-hydroxybenzamide trifluoroacetate

Downstream raw materials:

2-[3-endo-(3-carbamoyl-2-hydroxyphenyl)-8-aza-bicyclo[3.2.1]oct-8-yl]-ethyl-(2-ethylbutyl)-carbamic acid tert-butyl ester

3-endo-(8-(2-[(4,4-difluorocyclohexylmethyl)amino]-ethyl)-8-azabicyclo[3.2.1]oct-3-yl)-2-hydroxybenzamide

2-[3-endo-(3-carbamoyl-2-hydroxyphenyl)-8-azabicyclo[3.2.1]oct-8-yl]-ethyl-(2,2-dimethyl-propyl)carbamic acid benzyl ester

2-[3-endo-(3-carbamoyl-2-hydroxy-phenyl)-8-aza-bicyclo[3.2.1]oct-8-yl]-ethyl-(4,4-difluoro-cyclohexylmethyl)-carbamic acid benzyl ester

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