methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate

Base Information

Chemical Name:methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate
CAS No.:62653-84-3
Molecular Formula:C₁₃H₂₂O₃
Molecular Weight:226.316
Hs Code.:

Synonyms:methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate

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Technology Process of methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate

There total 2 articles about methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 205042-13-3
[(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxy)-2-(2-oxo-ethyl)-cyclopentyl]-acetic acid methyl ester

: 62653-84-3
methyl cucurbate methyl {(1R,2S,3S)-3-hydroxy-2-[(2Z)-pent-2-en-1-yl]cyclopentyl}acetate

: [(S)-3-(tert-Butyl-diphenyl-silanyloxy)-2-((Z)-pent-2-enyl)-cyclopentyl]-acetic acid methyl ester

Guidance literature:: With TBF; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00069-6

Reference yield:

: 110-71-4
1,2-dimethoxyethane

: [(1S,3R)-3-Hydroxy-2-(2-oxo-ethyl)-cyclopentyl]-acetic acid methyl ester

: 53403-88-6,54595-00-5,54595-10-7,81371-65-5,113351-08-9,128820-28-0,137431-74-4,137431-94-8,143292-39-1,807630-26-8
(1RS,2RS,3RS)-8-((2Z)-pentenyl)-2-oxaicyclo<3.2.1>octan-3-one

: 51388-61-5,53369-28-1,54595-02-7,54595-03-8,54595-04-9,54595-05-0,62653-84-3,113427-78-4,117179-89-2,121468-37-9,121468-38-0,128777-72-0,128820-29-1,139560-27-3,143234-99-5,146143-03-5,146143-05-7
[(1R,2S,3S)-3-Hydroxy-2-((Z)-pent-2-enyl)-cyclopentyl]-acetic acid methyl ester

Guidance literature:: With n-butyllithium; n-propylphosphonium bromide; Yield given. Multistep reaction. Yields of byproduct given; 1) 0 deg C, 1 h; 30 min; 2) RT;