2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene

Base Information

• Chemical Name: 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene
• CAS No.: 131380-97-7
• Molecular Formula: C₃₂H₂Cl₂₄
• Molecular Weight: 1237.24
• Mol file: 131380-97-7.mol

Synonyms:2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene

Chemical Property of 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene

There total 2 articles about 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

pentachlorobenzene (608-93-5) + 1,2,3,5-tetrachloro-4,6-bis-dichloromethyl-benzene (2136-96-1) → αH-Pentadecachlorotriphenylmethane (33240-61-8) + 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene (131380-97-7)

Guidance literature:

With aluminium trichloride; at 140 ℃; for 6h;

Reference yield:

1,2,3,5-tetrachlorobenzene (634-90-2) → 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene (131380-97-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / AlCl₃ / 9 h / Heating

2: 36 percent / AlCl₃ / 6 h / 140 °C

With aluminium trichloride;

Reference yield:

2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylene (131380-97-7) → 2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylyl radical (131380-98-8)

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; chloranil; Yield given. Multistep reaction; 1.) THF, RT, 3 h, 2.) RT, 2 h;

upstream raw materials:

pentachlorobenzene

1,2,3,5-tetrachloro-4,6-bis-dichloromethyl-benzene

1,2,3,5-tetrachlorobenzene

Downstream raw materials:

2,4,5,6-tetrachloro-α,α,α',α'-tetrakis(pentachlorophenyl)-m-xylyl radical