1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene

Base Information

• Chemical Name: 1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene
• CAS No.: 33240-61-8
• Molecular Formula: C₁₉HCl₁₅
• Molecular Weight: 761.012
• NSC Number: 168684
• DSSTox Substance ID: DTXSID90304983
• Nikkaji Number: J401.928H
• Wikidata: Q82051369
• Mol file: 33240-61-8.mol

Synonyms:4070-01-3;1-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene;1-[BIS(2,3,4,5,6-PENTACHLOROPHENYL)METHYL]-2,3,4,5,6-PENTACHLORO-BENZE NE;NSC168684;tris(pentachlorphenyl)methane;Tris(pentachlorophenyl)methane;SCHEMBL13703708;DTXSID90304983;NSC-168684;33240-61-8;1,1',1''-Methanetriyltris(pentachlorobenzene)

Chemical Property of 1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene

Chemical Property:

• XLogP3: 14.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 759.531765
• Heavy Atom Count: 34
• Complexity: 560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1(=C(C(=C(C(=C1Cl)Cl)Cl)Cl)Cl)C(C2=C(C(=C(C(=C2Cl)Cl)Cl)Cl)Cl)C3=C(C(=C(C(=C3Cl)Cl)Cl)Cl)Cl

Technology Process of 1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene

There total 9 articles about 1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,4,5,6-pentachlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

18-C-6-potassium perchlorotriphenylmethide complex (1/1) → αH-Pentadecachlorotriphenylmethane (33240-61-8)

Guidance literature:

With hydrogenchloride; In dichloromethane; for 1h;

DOI:10.1016/0022-328X(85)80410-1

Reference yield: 85.0%

pentachlorobenzene (608-93-5) + α-chlorobis(pentachlorophenyl)methane (33119-38-9) → αH-Pentadecachlorotriphenylmethane (33240-61-8)

Guidance literature:

With aluminium trichloride; at 90 ℃; for 2.5h;

DOI:10.1055/s-1986-31479

Reference yield: 80.0%

chloroform (67-66-3,8013-54-5) + pentachlorobenzene (608-93-5) → αH-Pentadecachlorotriphenylmethane (33240-61-8)

Guidance literature:

With aluminium trichloride; at 150 ℃; for 2.5h;

DOI:10.1055/s-1986-31479

upstream raw materials:

chloroform

pentachlorobenzene

α-chlorobis(pentachlorophenyl)methane

1,2,3,5-tetrachloro-4,6-bis-dichloromethyl-benzene

Downstream raw materials:

Tetra-n-butylammonium perchlorotriphenylmethide

perchlorotriphenylmethyl radical