C₂₃H₂₇F₂N₇O₃S

Base Information

Chemical Name:C₂₃H₂₇F₂N₇O₃S
CAS No.:1383744-74-8
Molecular Formula:C₂₃H₂₇F₂N₇O₃S
Molecular Weight:519.575
Hs Code.:

C<sub>23</sub>H<sub>27</sub>F<sub>2</sub>N<sub>7</sub>O<sub>3</sub>S

Synonyms:C₂₃H₂₇F₂N₇O₃S

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Chemical Property of C₂₃H₂₇F₂N₇O₃S

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Technology Process of C₂₃H₂₇F₂N₇O₃S

There total 9 articles about C₂₃H₂₇F₂N₇O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6704-31-0
oxetan-3-one

: 1383744-73-7
C₂₀H₂₃F₂N₇O₂S

: 1383744-74-8
C₂₃H₂₇F₂N₇O₃S

Guidance literature:: oxetan-3-one; C₂₀H₂₃F₂N₇O₂S; With acetic acid; In N,N-dimethyl-formamide; for 0.0166667h;

With sodium tris(acetoxy)borohydride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 3896-29-5
N-(2,6-difluorophenyl)acetamide

: 1383744-74-8
C₂₃H₂₇F₂N₇O₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium nitrate; sulfuric acid / 2 h / -10 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / autoclave

3.1: pyridine / dichloromethane / 16 h / 20 °C

4.1: hydrogenchloride / ethanol; water / 2 h / 80 °C

5.1: trifluoroacetic acid; sodium nitrite / 0.5 h / 0 °C

5.2: 0.25 h

6.1: potassium fluoride / methanol / 3 h / 20 °C

6.2: 16 h / 45 °C

7.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

8.1: acetic acid / N,N-dimethyl-formamide / 0.02 h

8.2: 18 h / 20 °C

With pyridine; hydrogenchloride; potassium fluoride; sulfuric acid; hydrogen; acetic acid; potassium nitrate; trifluoroacetic acid; sodium nitrite; palladium 10% on activated carbon; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 25892-08-4
N-(2,6-difluoro-3-nitrophenyl)acetamide

: 1383744-74-8
C₂₃H₂₇F₂N₇O₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / autoclave

2.1: pyridine / dichloromethane / 16 h / 20 °C

3.1: hydrogenchloride / ethanol; water / 2 h / 80 °C

4.1: trifluoroacetic acid; sodium nitrite / 0.5 h / 0 °C

4.2: 0.25 h

5.1: potassium fluoride / methanol / 3 h / 20 °C

5.2: 16 h / 45 °C

6.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

7.1: acetic acid / N,N-dimethyl-formamide / 0.02 h

7.2: 18 h / 20 °C

With pyridine; hydrogenchloride; potassium fluoride; hydrogen; acetic acid; trifluoroacetic acid; sodium nitrite; palladium 10% on activated carbon; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;