10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

Base Information

Chemical Name:10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one
CAS No.:662723-18-4
Molecular Formula:C₃₂H₂₇NO₄
Molecular Weight:489.571
Hs Code.:

Synonyms:10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

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Chemical Property of 10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

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Technology Process of 10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

There total 10 articles about 10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 77-78-1
dimethyl sulfate

: 662723-16-2
10-hydroxy-10-[7-methoxy-3-(2-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

: 662723-18-4
10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In benzene; at 20 ℃;

Reference yield: 10.0%

: 108-24-7
acetic anhydride

: 662723-20-8
10-acetoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

: acetic acid 10-(3-methoxymethyl-6-oxo-6H-benzo[c]chromen-4-yl)-anthracen-9-yl ester

: 662723-18-4
10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

Guidance literature:: 10-acetoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one; With cyclohexa-1,4-diene; trifluoroacetic acid; In methanol; at 37 ℃; for 1h;

acetic anhydride; With pyridine; at 20 ℃;

Reference yield:

: 180713-44-4
2-[(pivaloyloxy)methyl]benzaldehyde

: 662723-18-4
10-methoxy-10-[7-methoxy-3-(2-N,N-dimethylaminocarbonylphenyl)hept-3-ene-1,5-diynyl]-10H-anthracen-9-one

Guidance literature:: Multi-step reaction with 11 steps

1.1: 44.6 g / tetrahydrofuran / 0.5 h / 0 °C

2.1: 87 percent / CrO₃; aq. H₂SO₄ / acetone / 0 - 20 °C

3.1: 73 percent / Zn / tetrahydrofuran / 0.5 h / Heating

4.1: 81 percent / triethylamine; methanesulfonyl chloride / CH₂Cl₂ / 2 h / 0 °C

5.1: 52 percent / EtMgBr / tetrahydrofuran; CH₂Cl₂ / Heating

6.1: 80 percent / K₂CO₃ / methanol / 4 h / 20 °C

7.1: MnO₂ / benzene / 2 h / 20 °C

8.1: 662 mg / 2-methyl-2-butene; NaClO₂; NaH₂PO₄*H₂O / 2-methyl-propan-2-ol; H₂O / 2 h / 20 °C

9.1: 81 percent / N,N-diisopropylethylamine; dicyano diethylphosphate / tetrahydrofuran / 2 h / 0 °C

10.1: 82 percent / DMAP; EDC / CH₂Cl₂ / 0 °C

11.1: 1,4-cyclohexadiene; aq. trifluoroacetic acid / methanol / 1 h / 37 °C

11.2: 71 percent / pyridine / 20 °C

With chromium(VI) oxide; dmap; manganese(IV) oxide; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; cyclohexa-1,4-diene; dicyano diethylphosphate; sulfuric acid; ethylmagnesium bromide; potassium carbonate; methanesulfonyl chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetone; tert-butyl alcohol; benzene;