(2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

Base Information

• Chemical Name: (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane
• CAS No.: 440368-62-7
• Molecular Formula: C₂₂H₂₆N₄O₈
• Molecular Weight: 474.47

Synonyms:(2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

Chemical Property of (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

Chemical Property:

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Technology Process of (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

There total 1 articles about (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

Glyoxal (131543-46-9,107-22-2) + (1S,2S)-2-(dimethylamino)1-(4-nitrophenyl)propane-1,3-diol hydrochloride + (1S,2S)-2-amino-1-(4-nitrophenyl)propane-1,3-diol hydrochloride (19534-26-0) → (2R,2'R,4S,4'S,5S,5'S)-5-amino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane (440368-60-5) + (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane (440368-62-7) + (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-dimethylamino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane

Guidance literature:

Glyoxal; (1S,2S)-2-amino-1-(4-nitrophenyl)propane-1,3-diol hydrochloride; With sulfuric acid; at 0 ℃; for 15h;

(1S,2S)-2-(dimethylamino)1-(4-nitrophenyl)propane-1,3-diol hydrochloride; at 0 - 20 ℃;

DOI:10.1002/ejoc.200700847

Reference yield: 45.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + (2R,2'R,4S,4'S,5S,5'S)-5-dimethylamino-4-(4-nitrophenyl)-2-[5'-amino-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-1,3-dioxane (440368-62-7) → 2-chloro-4,6-bis{(2R,4S,5S)-2-[(2'R,4'S,5'S)-5'-(dimethylamino)-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-4-(4-nitrophenyl)-1,3-dioxan-5-ylamino}-s-triazine (1042072-85-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 48h; Reflux;

DOI:10.1002/ejoc.200700847

upstream raw materials:

Glyoxal

(1S,2S)-2-amino-1-(4-nitrophenyl)propane-1,3-diol hydrochloride

Downstream raw materials:

2-chloro-4,6-bis{(2R,4S,5S)-2-[(2'R,4'S,5'S)-5'-(dimethylamino)-4'-(4'-nitrophenyl)-1',3'-dioxan-2'-yl]-4-(4-nitrophenyl)-1,3-dioxan-5-ylamino}-s-triazine

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