3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

Base Information

Chemical Name:3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester
CAS No.:85805-46-5
Molecular Formula:C₂₉H₂₈ClNO₇
Molecular Weight:537.997
Hs Code.:

Synonyms:3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

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Technology Process of 3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

There total 3 articles about 3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.4%

: 85805-45-4
2,6-Dibenzyloxyphenyliminomalonsaeurediethylester

: 79-04-9
chloroacetyl chloride

: 85805-46-5
3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

Guidance literature:: With triethylamine; In benzene; at 80 ℃; for 1h;
DOI:10.1002/ardp.19833160417

Reference yield:

: 61999-92-6
2,6-di(benzyloxy)aniline

: 85805-46-5
3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / toluene / 2 h / Heating

2: 76.4 percent / Et₃N / benzene / 1 h / 80 °C

With triethylamine; In toluene; benzene;
DOI:10.1002/ardp.19833160417

Reference yield:

: 609-09-6
Diethyl ketomalonate

: 85805-46-5
3-Chlor-1-(2,6-dibenzyloxyphenyl)-4-oxo-azetidin-2,2-dicarbonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / toluene / 2 h / Heating

2: 76.4 percent / Et₃N / benzene / 1 h / 80 °C

With triethylamine; In toluene; benzene;
DOI:10.1002/ardp.19833160417