ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

Base Information

Chemical Name:ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate
CAS No.:172896-68-3
Molecular Formula:C₂₃H₂₇ClN₂O₃S
Molecular Weight:446.998
Hs Code.:

Synonyms:ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

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Technology Process of ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

There total 2 articles about ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 172896-64-9
N-tert-butyl-N-phenylthiocarbamoylacetic acid

: 172896-37-6
ethyl 5-chloro-2-(methylamino)benzoate

: 172896-68-3
ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

Guidance literature:: With pyridine; 4 A molecular sieve; pivaloyl chloride; In dichloromethane; at -20 - 20 ℃;
DOI:10.1002/jhet.5570390427

Reference yield:

: 64-17-5
ethanol

: 14529-12-5
6-chloro-N-methylisatoic anhydride

: 172896-64-9
N-tert-butyl-N-phenylthiocarbamoylacetic acid

: 172896-68-3
ethyl 2-{[2-(tert-butyl-phenyl-thiocarbamoyl)-acetyl]-methylamino}-5-chlorobenzoate

Guidance literature:: ethanol; 6-chloro-N-methylisatoic anhydride; With sodium ethanolate; Heating;

N-tert-butyl-N-phenylthiocarbamoylacetic acid; With pyridine; pivaloyl chloride; In dichloromethane; at 20 ℃;
DOI:10.1016/S0960-894X(02)00377-3