6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Base Information

Chemical Name:6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione
CAS No.:14529-12-5
Molecular Formula:C9H6ClNO3
Molecular Weight:211.605
Hs Code.:
European Community (EC) Number:238-551-6
DSSTox Substance ID:DTXSID90162964
Nikkaji Number:J67.821J
Wikidata:Q72454132
ChEMBL ID:CHEMBL2146654
Mol file:14529-12-5.mol

Synonyms:14529-12-5;6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione;5-CHLORO-N-METHYLISATOIC ANHYDRIDE;6-chloro-1-methyl-3,1-benzoxazine-2,4-dione;6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione;6-Chloro-N-methyl IA;BRN 0613893;EINECS 238-551-6;2H-3,1-BENZOXAZINE-2,4(1H)-DIONE, 6-CHLORO-1-METHYL-;6-chloro-1-methyl-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione;N-methyl-5-chloroisatoic anhydride;SCHEMBL607256;CHEMBL2146654;DTXSID90162964;AMY23289;5-Chloro-N-methyl Isatoic anhydride;AKOS002664950;LS-41763;FT-0645822;EN300-235715;F87126;6-chloranyl-1-methyl-3,1-benzoxazine-2,4-dione;A808345;A1-47366;F1943-0050

Suppliers and Price of 6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
50mg
$ 65.00

Crysdot
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione 95+%
5g
$ 823.00

Chemenu
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione 95%
5g
$ 777.00

Biosynth Carbosynth
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
5 g
$ 1250.00

Biosynth Carbosynth
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
2 g
$ 800.00

Biosynth Carbosynth
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
500 mg
$ 400.00

Biosynth Carbosynth
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
250 mg
$ 300.00

Biosynth Carbosynth
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
1 g
$ 600.00

American Custom Chemicals Corporation
6-CHLORO-1-METHYL-1H-BENZO[D][1,3]OXAZINE-2,4-DIONE 95.00%
5MG
$ 502.95

Alichem
6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione
1g
$ 400.00

Total 83 raw suppliers

Chemical Property of 6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

Chemical Property:

Vapor Pressure:5.57E-05mmHg at 25°C
Melting Point:113 °C
Refractive Index:1.597
Boiling Point:346.94 °C at 760 mmHg
PKA:-3.11±0.20(Predicted)
Flash Point:163.623 °C
PSA：52.21000
Density:1.477 g/cm³
LogP:1.14510
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:211.0036207
Heavy Atom Count:14
Complexity:281

Purity/Quality:

99% ^*data from raw suppliers

6-Chloro-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)C(=O)OC1=O

Technology Process of 6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione

There total 13 articles about 6-Chloro-1-methyl-2H-3,1-benzoxazine-2,4(1H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4743-17-3
5-Chloroisatoic anhydride

: 74-88-4
methyl iodide

: 14529-12-5
6-chloro-N-methylisatoic anhydride

Guidance literature:: In ice-water; ISOPROPYLAMIDE;

Reference yield: 78.0%

: 201230-82-2
carbon monoxide

: 932-96-7
N-methyl(p-chloroaniline)

: 14529-12-5
6-chloro-N-methylisatoic anhydride

Guidance literature:: With oxygen; copper diacetate; palladium diacetate; potassium iodide; Trimethylacetic acid; In acetonitrile; at 60 ℃; under 760.051 Torr; regioselective reaction;
DOI:10.1021/ja308976x

Reference yield: 72.0%

: 4743-17-3
5-Chloroisatoic anhydride

: 74-83-9
methyl bromide

: 14529-12-5
6-chloro-N-methylisatoic anhydride

Guidance literature:: 5-Chloroisatoic anhydride; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

methyl bromide; In N,N-dimethyl-formamide; for 18h;
DOI:10.1016/j.bmc.2012.08.049