C₂₈H₃₇BPOLi

Base Information

• Chemical Name: C₂₈H₃₇BPOLi
• CAS No.: 118496-22-3
• Molecular Formula: C₂₈H₃₇BLiOP
• Molecular Weight: 438.327
• Mol file: 118496-22-3.mol

Synonyms:C₂₈H₃₇BPOLi

Chemical Property of C₂₈H₃₇BPOLi

Chemical Property:

Purity/Quality:

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Technology Process of C₂₈H₃₇BPOLi

There total 1 articles about C₂₈H₃₇BPOLi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.1%

dimesitylfluoroborane (436-59-9) + phenylphosphane (638-21-1) → C28H37BPOLi (118496-22-3)

Guidance literature:

With n-BuLi; In diethyl ether; hexane; byproducts: LiF; stirring by cooling then at room temp. 1.5 h, then cooling, addn. of Mes2BF stirring 5 h at room temp. addn. of n-BuLi again by cooling then stirring at room temp. for 2 h; filtration, extn. with pentane, volume reduced, washing with hexane;

DOI:10.1021/ja00022a034

upstream raw materials:

dimesitylfluoroborane

phenylphosphane