13-methoxy-8H-dibenzoquinolizin-8-one

Base Information

• Chemical Name: 13-methoxy-8H-dibenzoquinolizin-8-one
• CAS No.: 81750-93-8
• Molecular Formula: C₁₈H₁₃NO₂
• Molecular Weight: 275.307

Synonyms:13-methoxy-8H-dibenzoquinolizin-8-one

Chemical Property of 13-methoxy-8H-dibenzoquinolizin-8-one

Chemical Property:

Purity/Quality:

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Technology Process of 13-methoxy-8H-dibenzoquinolizin-8-one

There total 2 articles about 13-methoxy-8H-dibenzoquinolizin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methanol (67-56-1) + tetramethyl 2,2'-phthaloylbis(1,2-dihydro-1-isoquinolylphosphonate) → isoquinoline (119-65-3) + 13-methoxy-8H-dibenzoquinolizin-8-one (81750-93-8) + dimethyl 2--1,2-dihydro-1-isoquinolylphosphonate (81750-90-5)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; Mechanism; Product distribution; 1) - 70 deg C, 0.5 h, 2) room temperature, overnight;

DOI:10.1246/bcsj.57.2333

Reference yield: 84.0%

methanol (67-56-1) + tetraethyl 2,2'-phthaloylbis(1,2-dihydro-1-isoquinolylphosphonate) → isoquinoline (119-65-3) + phthalic acid dimethyl ester (131-11-3,64441-70-9) + 13-methoxy-8H-dibenzoquinolizin-8-one (81750-93-8) + diethyl 2--1,2-dihydro-1-isoquinolylphosphonate

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; Mechanism; Product distribution; 1) - 70 deg C, 0.5 h, 2) room temperature, overnight;

DOI:10.1246/bcsj.57.2333

upstream raw materials:

methanol

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