2-benzoyl-3-phenylbutanoic acid ethyl ester

Base Information

Chemical Name:2-benzoyl-3-phenylbutanoic acid ethyl ester
CAS No.:891821-80-0
Molecular Formula:C₁₉H₂₀O₃
Molecular Weight:296.366
Hs Code.:

Synonyms:2-benzoyl-3-phenylbutanoic acid ethyl ester

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Chemical Property of 2-benzoyl-3-phenylbutanoic acid ethyl ester

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Technology Process of 2-benzoyl-3-phenylbutanoic acid ethyl ester

There total 3 articles about 2-benzoyl-3-phenylbutanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-85-1,13323-81-4
1-Phenylethanol

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 891821-80-0
2-benzoyl-3-phenylbutanoic acid ethyl ester

Guidance literature:: ethyl 3-oxo-3-phenylpropionate; With pentafluorophenylboronic acid; oxalic acid; In nitromethane; at 20 - 25 ℃; for 0.0833333h;

1-Phenylethanol; In nitromethane; at 90 ℃; for 16h;
DOI:10.1021/acs.orglett.0c02736

Reference yield: 60.0%

: 98-85-1,13323-81-4
1-Phenylethanol

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 891821-80-0
2-benzoyl-3-phenylbutanoic acid ethyl ester

: 93-96-9
bis(1-phenylethyl)ether

Guidance literature:: With Amberlyst-15; at 80 ℃; for 6h; optical yield given as %de; Ionic liquid;
DOI:10.1016/j.tetlet.2009.11.122

Reference yield:

: 100-52-7
benzaldehyde

: 891821-80-0
2-benzoyl-3-phenylbutanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 6.5 h / 0 - 25 °C / Inert atmosphere

2.1: pentafluorophenylboronic acid; oxalic acid / nitromethane / 0.08 h / 20 - 25 °C

2.2: 16 h / 90 °C

With pentafluorophenylboronic acid; oxalic acid; In tetrahydrofuran; nitromethane;
DOI:10.1021/acs.orglett.0c02736