3-Amino-2-iodobenzenemethanol

Base Information

Chemical Name:3-Amino-2-iodobenzenemethanol
CAS No.:158616-09-2
Molecular Formula:C₇H₈INO
Molecular Weight:249.051
Hs Code.:
DSSTox Substance ID:DTXSID601307134

Synonyms:158616-09-2;3-Amino-2-iodobenzenemethanol;3-Amino-2-iodobenzyl alcohol;DTXSID601307134

Suppliers and Price of 3-Amino-2-iodobenzenemethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Amino-2-iodobenzenemethanol

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:248.96506
Heavy Atom Count:10
Complexity:110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)N)I)CO

Technology Process of 3-Amino-2-iodobenzenemethanol

There total 1 articles about 3-Amino-2-iodobenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5398-69-6
2-iodo-3-nitrobenzoic acid

: 158616-09-2
3-amino-2-iodobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃*THF / tetrahydrofuran / 0 deg C, 1 h; r.t., 3 h

2: Fe, HCl / acetic acid; ethanol / 3 h / Heating

With hydrogenchloride; borane-THF; iron; In tetrahydrofuran; ethanol; acetic acid;
DOI:10.1016/S0040-4020(01)85078-X

Reference yield: 80.0%

: 158616-09-2
3-amino-2-iodobenzyl alcohol

: 74-88-4
methyl iodide

: 3-(dimethylamino)-2-iodobenzyl alcohol

Guidance literature:: With potassium carbonate; In acetonitrile; at 50 ℃; for 24h;
DOI:10.1039/b708306h

Reference yield:

: 158616-09-2
3-amino-2-iodobenzyl alcohol

: 156263-58-0
2-iodo-3-(tert-butyldimethylsiloxymethyl)-N-allylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole, DMAP / dimethylformamide / 18 h / Ambient temperature

2: 74 percent / LDA / tetrahydrofuran / -78 deg C, 30 min; r.t., 4 h

With 1H-imidazole; dmap; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85078-X