N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

Base Information

Chemical Name:N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide
CAS No.:1321620-89-6
Molecular Formula:C₃₀H₂₅N₅O₂
Molecular Weight:487.561
Hs Code.:

N<SUP>2</SUP>,N<SUP>5</SUP>-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

Synonyms:N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

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Chemical Property of N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

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Technology Process of N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

There total 3 articles about N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.7%

: 1824-81-3
2-Amino-6-methylpyridine

: 3,4-diphenyl-1H-pyrrole-2,5-dicarbonyl dichloride

: 1321620-89-6
N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 20.5h; Inert atmosphere;
DOI:10.1021/jo201191x

Reference yield:

: 156-06-9
2-oxo-3-(phenyl)propionic acid

: 1321620-89-6
N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

1.3: 24 h / Inert atmosphere

2.1: thionyl chloride / Reflux

3.1: triethylamine / tetrahydrofuran / 20.5 h / 0 - 20 °C / Inert atmosphere

With n-butyllithium; thionyl chloride; triethylamine; In tetrahydrofuran; hexane;
DOI:10.1021/jo201191x

Reference yield:

: 1632-49-1
3,4-diphenyl-1H-pyrrole-2,5-dicarboxylic acid

: 1321620-89-6
N²,N⁵-bis(6-methylpyridin-2-yl)-3,4-diphenyl-1H-pyrrole-2,5-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Reflux

2: triethylamine / tetrahydrofuran / 20.5 h / 0 - 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo201191x