sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

Base Information

Chemical Name:sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate
CAS No.:1416063-48-3
Molecular Formula:C₈H₃F₄O₅S*Na
Molecular Weight:310.158
Hs Code.:

Synonyms:sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

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Technology Process of sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

There total 1 articles about sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 64-19-7,77671-22-8
acetic acid

: 2,3,5,6-tetrafluoro-4-hydroxybenzene sulfonic acid sodium salt

: 1416063-48-3
sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

Guidance literature:: With dicyclohexyl-carbodiimide; In acetone; at 20 ℃; for 20h;

Reference yield: 30.0%

: 375-22-4
heptafluorobutyric Acid

: 1416063-48-3
sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate

: 4146-30-9,25389-98-4,28002-70-2,34289-38-8,92283-95-9
neomycin B trisulfate

: N⁶(V)-acetyl neomycin B*5HFBA

: N-(5-amino-6-{4,6-diamino-2-[4-(3-amino-6-aminomethyl-4,5-dihydroxy-tetrahydro-pyran-2-yloxy)-3-hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yloxy]-3-hydroxy-cyclohexyloxy}-3,4-dihydroxy-tetrahydro-pyran-2-ylmethyl)-acetamide

Guidance literature:: neomycin B trisulfate; With 5′-GGACUGGGCGAGAAGUUUAGUCC-3′; In aq. phosphate buffer; at 20 ℃; for 0.5h;

sodium 4-(acetoxy)-2,3,5,6-tetrafluorobenzenesulfonate; In aq. phosphate buffer; N,N-dimethyl-formamide; at 20 ℃; for 24h;

heptafluorobutyric Acid; regioselective reaction; Further stages;
DOI:10.1039/d0ob02104k