C₃₂H₆₂O₆Si₂

Base Information

Chemical Name:C₃₂H₆₂O₆Si₂
CAS No.:1351977-17-7
Molecular Formula:C₃₂H₆₂O₆Si₂
Molecular Weight:599.012
Hs Code.:

C<sub>32</sub>H<sub>62</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₂H₆₂O₆Si₂

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Chemical Property of C₃₂H₆₂O₆Si₂

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Technology Process of C₃₂H₆₂O₆Si₂

There total 16 articles about C₃₂H₆₂O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1351977-07-5
C₄₂H₆₉NO₈Si₂

: 1351977-17-7
C₃₂H₆₂O₆Si₂

Guidance literature:: With lithium borohydride; ethanol; In tetrahydrofuran; diethyl ether; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol203130b

Reference yield:

: 1351977-06-4
(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

: 1351977-17-7
C₃₂H₆₂O₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: lithium borohydride; ethanol / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Inert atmosphere

With lithium borohydride; ethanol; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Aldol condensation / 1.2: Aldol condensation;
DOI:10.1021/ol203130b

Reference yield:

: C₃₁H₅₈O₆Si₂

: 1351977-17-7
C₃₂H₆₂O₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 23 °C / Inert atmosphere

3.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 °C / Inert atmosphere

4.1: lithium borohydride; ethanol / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Inert atmosphere

With pyridine; lithium borohydride; ethanol; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 3.1: Aldol condensation / 3.2: Aldol condensation;
DOI:10.1021/ol203130b