N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide

Base Information

• Chemical Name: N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide
• CAS No.: 1024005-32-0
• Molecular Formula: C₂₁H₂₃F₂N₃O₂
• Molecular Weight: 387.429

Synonyms:N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide

Chemical Property of N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide

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Technology Process of N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide

There total 1 articles about N₁-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-diene-3-yl-methoxymethaneimine (1024005-29-5) + pivaloyl chloride (3282-30-2) → N1-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide (1024005-32-0)

Guidance literature:

With triethylamine; In toluene; at 0 - 35 ℃; for 48h;

Reference yield: 87.0%

N1-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide (1024005-32-0) → 5-[5-(tert-butyl)-1H-1,2,4-triazol-3-yl]-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene (1024003-84-6)

Guidance literature:

With hydrazine; In methanol; at 20 - 35 ℃; for 2h;

Reference yield: 85.0%

N1-{1-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-yl]-1-methoxymethylidene}-2,2-dimethyl propanamide (1024005-32-0) → 5-(tert-butyl)-3-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3yl]-1,2,4-oxadiazole (1024003-85-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium methylate; In methanol; at 20 - 35 ℃; for 12.25h;

upstream raw materials:

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-diene-3-yl-methoxymethaneimine

pivaloyl chloride

Downstream raw materials:

5-[5-(tert-butyl)-1H-1,2,4-triazol-3-yl]-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene

5-(tert-butyl)-3-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3yl]-1,2,4-oxadiazole

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