3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

Base Information

Chemical Name:3-phenylprop-2-yne-1,1-diyl gem-dibenzoate
CAS No.:1260421-92-8
Molecular Formula:C₂₃H₁₆O₄
Molecular Weight:356.378
Hs Code.:

Synonyms:3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

Suppliers and Price of 3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

There total 1 articles about 3-phenylprop-2-yne-1,1-diyl gem-dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 2579-22-8
Phenylpropargyl aldehyde

: 93-97-0
benzoic acid anhydride

: 1260421-92-8
3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

Guidance literature:: With iron(III) chloride; In dichloromethane; at 20 ℃; for 6h; chemoselective reaction;
DOI:10.1016/j.tetlet.2010.10.013

Reference yield: 74.0%

: 1260421-92-8
3-phenylprop-2-yne-1,1-diyl gem-dibenzoate

: 925-90-6
ethylmagnesium bromide

: 1260422-01-2
3-phenylpenta-1,2-dienyl benzoate

Guidance literature:: ethylmagnesium bromide; With copper(l) iodide; lithium bromide; In tetrahydrofuran; tert-butyl methyl ether; at -10 ℃; Inert atmosphere;

3-phenylprop-2-yne-1,1-diyl gem-dibenzoate; In tetrahydrofuran; tert-butyl methyl ether; at -10 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.10.013